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Advances and recent applications in LC-MS and HPLC / Quazi Syed Azharuddin [and seven others].
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Title:Advances and recent applications in LC-MS and HPLC / Quazi Syed Azharuddin [and seven others].
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Author/Creator:Azharuddin, Quazi Syed, author.
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Published/Created:Amsterdam : Elsevier, [2015]
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Holdings
Holdings Record Display
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Location:WOODWARD LIBRARY stacksWhere is this?
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Call Number: QP519.9.L55 A94 2015
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Number of Items:1
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Status:Available
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Location:WOODWARD LIBRARY stacksWhere is this?
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Library of Congress Subjects:Liquid chromatography.
Mass spectrometry.
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Medical Subjects: Chromatography, Liquid--methods.
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Description:vii, 86 pages ; 23 cm
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Notes:Includes bibliographical references.
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ISBN:9780128042076 paperback
0128042079 paperback
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Contents:Machine generated contents note: ch. 1 Introduction: Liquid Chromatography/Mass Spectrometry
Definitions
Fundamentals of LC/MS
Application of LC/MS
ch. 2 Construction of High-Performance Liquid Chromatography
Construction of the HPLC System
Microcomponents of HPLC
Tubing and Design of HPLC
ch. 3 Advances and Recent Applications in LC/MS
Determination of Lipophilicity in Preservative Drugs
Preservative Drugs: Methylparaben
Detection of Compounds
Study of Complex Biologic Molecules
Identification of Impurities and Metabolites
Analysis of Flammable Materials
Study of Toxicology and Drugs
Analysis of Clinical Drugs
Analysis of Pesticides
ch. 4 Column and Distribution Modes
Stainless Steel Columns
Column Packing Substance
Selectivity in Normal Phase
Bonded-Phase Silica
Effect of the Mobile Phase
Optimizing Separation of Ionic and Nonionic Reversed Phase
Zirconium Packing Separation Mode Columns
Polymeric Bonded-Phase Columns
Ion-Exchange Columns
ch. 5 Column Safety Procedures in HPLC
Safety Procedures in HPLC
Injector Along with Pipe Washing
Gradient Routine Checking
Water with Solvent Cleanup
Silica Column Cleanup
Zirconium Column Cleaning
Polymeric Column Safety
ch. 6 Solution Preparation
Preparation Solvent of HPLC
Controlling the Selectivity of pH
Solution Preparation
Cartridge Column Cleaning
Effect of Concentration
Development of Isocratic and Gradient Elution
Computer-Assisted Development
ch. 7 Basic Components LC/MS
Ionization Source
Analyzer with Ion Detector Development
Vacuum Pumps
Peak Detection
ch. 8 Solvent Removal Process for Liquid Chromatography and the Mass Spectrometer
Elution Solvent and Ionization
Atmospheric Pressure Ionization Interfaces
ES Ionization Interface
IS Interface
ch. 9 Mass Analyzer Instrumentation Technique
Quadrupole
Mass Spectrometers Analyzers Instrument
Mass Spectrometers Ion Trap Analyzer
Time of Flight (TOF)
Fourier Transform Mass Spectrometry (FT-MS)
ch. 10 Mass Spectrometer Operating Procedure
Mass Spectrometer Vacuum Pump
MS Vacuum Analysis
Pump Servicing
Mass Spectrometer Operating Process
Mass Spectrophotometer Calibration
Instrumentation Cleaning Process
ch. 11 Proteins Analysis and LC/MS
Determination of Protein Molecular Weight
Protein Study by Two-Dimensional GEP
Analysis of Peptide Structures
Transient Peptides and Buildup Proteins.